2-chloromethylthiophene
2-Chloromethylthiophene is used as an intermediate to 1-(2-thienyl)-2-Propanone. In a 2-l. beaker surrounded by an ice-salt bath , and fitted with a mechanical stirrer and a thermometer, are placed 420 g. (392 ml., 5 moles) of thiophene and 200 ml. of concentrated hydrochloric acid. A rapid stream of hydrogen chloride is passed continuously into the mixture with vigorous stirring. When the temperature reaches 0°, 500 ml. of 37% formaldehyde solution is added at a rate that will permit the temperature to remain below 5°. The addition requires about 4 hours. When all the formaldehyde solution has been added, the mixture is extracted with three 500-ml. portions of ether. The ether extracts are combined, washed successively with water and saturated sodium bicarbonate solution, and then dried over anhydrous calcium chloride. The solvent is removed by distillation, and the product is distilled under reduced pressure through a 50-cm. fractionating column. The product boiling at 73–75°/17 mm. is collected. The yield is 257–267 g. (40–41%) of a colorless oily liquid.
The Urban Dictionary Mug
I mollywopped someone with it and it didn’t break. Nice
Product was as advertised and arrived pretty quickly too! The person loved their gift!
The "Pink Flamingo" colour with white text on a pink background is the best selection for this fine phrase mug. May I suggest you also correct the misspelling of "delightfully" in the default option for a timeless gift.
As always, a great gift.
It looks great. I couldn't have been happier
It’s a mug I would never find in a souvenir shop. I’m a legend in my own home.
I am very please with the mug. Thank you!
ABSOLUTELY LOVED IT BUY IT RN
Was very happy with the customer service team when I had a question. They responded to my email quickly. The mug looks really cool, makes me laugh every time I use it and high quality. I’m in love with it. Thanks!
Haylee My name is haylee sullivan and the mug is describes everything about me and i would rate it at a 5 100% it is awesome
I’m right handed and would’ve liked it better if the handle was on right side with name facing forward instead of having verbiage facing front
girlfriend loved it :) - Ian's Girlfriend
the urge to buy it and write cum on it
Purchased this mug as a Christmas gift. Can’t wait to see the reaction!
This is to test if the Urban Dictionary store rating system is working and not showing fake 5 star reviews.
These are hilarious! Great gifts. Cost seems a bit high but i couldn’t resist.
It’s a great way to store my pencils.
I used this instead of condoms It didn’t work and now my nephew is my son
Ordering was very easy and the delivery to a different address then the billing address was done effortlessly with complete correct order. Was delivered before estimated date which was very exciting. Good job well done by all.
Funny stuff! I wish the mugs cost a bit less, I'd buy more. There's an almost unlimited supply of clever slang.
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